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Beilstein J. Org. Chem. 2015, 11, 514–523, doi:10.3762/bjoc.11.58
Graphical Abstract
Scheme 1: Synthetic route for the synthesis of the β-CD dimer with a free alkyne, allowing for subsequent sur...
Figure 1: MS spectra (2440–2500 Da) of the purified β-CD dimer.
Figure 2: Structure of fluorescent guest molecule, 2,6-ANS, used to probe host–guest interaction and two deri...
Figure 3: Illustration of potential 1:1 inclusion complexes of the β-CD dimer and 2,6-ANS.
Figure 4: (a) Steady-state fluorescence emission spectra of 50 µM 2,6-ANS in PBS (solid grey, smoothed), in t...
Figure 5: Region of interest of a ROESY (250 ms mixing time) showing cross peaks between the β-CD-dimer and 2...
Figure 6: Steady-state fluorescence titration of 2,6-ANS with β-CD dimer and parent β-CD in solution. 2,6-ANS...
Scheme 2: Synthetic route for the activation of silicon dioxide surfaces and the grafting of the β-CD dimer t...
Figure 7: (a) Steady-state TIRF emission spectra of 1 mM 2,6-ANS in PBS, recorded on a bare quartz slide (sol...
Beilstein J. Org. Chem. 2015, 11, 147–154, doi:10.3762/bjoc.11.14
Scheme 1: Reaction scheme for synthesis of azide-modified (S)-camptothecin.
Scheme 2: Cu(I)-catalyzed grafting of azide-modified (S)-camptothecin onto alkyne-modified dextran.
Figure 1: Titration of a) D70GP-CPT2 and b) D10GP-CPT1 by D70HPβ-CD at 298 K showing heat flow as a function ...
Figure 2: Fluorescence emission spectra of a) D70GPCPT and b) D10GPCPT recorded at different concentrations (...